Poster Presentation 14th Australian Peptide Conference 2022

Bioactive β- and γ-peptides (#412)

Zeinab Mahfouz 1 , Elisabeth K. Nyakatura 1 , Raheleh R. Araghi 1 , Jérémie Mortier 1 , Daniela Gjorgjevikj 1 , Nikolai Klishin 2 , Prof. Dr. Markus Wahl 1 , Prof. Dr. Heiko Möller 2 , Prof. Dr. Beate Koksch 1
  1. Department of Chemistry, Biochemistry and Pharmacy, Freie Universität Berlin, Berlin, Germany
  2. Institute of Chemistry, Universität Potsdam, Golm, Brandenburg, Germany

Selective disruption of interactions between helical domains emerged as attractive target for drug discovery.[1] However, protease susceptibility of natural peptides limits their clinical use as drugs. The design of foldamers strives to solve this problem of proteolytic degradation. Foldamers that are composed of β- and γ-amino acids mimic the self-assembly of native peptides.[2] Moreover, β/γ-peptides display similar H-bonding patterns to all-α-peptides. They present functional groups in a predictable manner[3] and the incorporation of β- and γ-amino acids leads to increased stability towards proteolytic degradation.[4]

In previous work, we investigated the interactions between an α/β/γ-chimera and all-α-peptides within the quaternary structure of a tetrameric coiled-coil motif.[1,5] In the course of this research, we presented a Cys/Phe-motif that selectively binds to the β/γ-module and exhibits comparable stability to their parental systems. MD simulations revealed the formation of an interstrand H-bond between the thiol-residue of Cys and the unbound backbone carbonyl of the β/γ-pentad sequence.[5] Our latest research focusses on structural studies such as crystallization strategies and NMR to examine the stabilizing effect of the interstrand H-bond of the heteroassembly. Furthermore, modular substitution of α-helical segments of the tetrameric coiled coil-system by β/γ-modules is performed and the obtained structural properties are investigated.

  1. [1] R. R. Araghi, C. Jäckel, H. Cölfen, M. Salwiczek, A. Völkel, S. C. Wagner, S. Wieczorek, C. Baldauf, B. Koksch, ChemBioChem 2010, 11, 335–339.
  2. [2] S. H. Gellman, Acc. Chem. Res. 1998, 31, 173–180.
  3. [3] T. Sawada, S. H. Gellman, J. Am. Chem. Soc. 2011, 133, 7336–7339.
  4. [4] D. Seebach, A. K. Beck, D. J. Bierbaum, 2004, 1, 1111–1239.
  5. [5] E. K. Nyakatura, R. Rezaei Araghi, J. Mortier, S. Wieczorek, C. Baldauf, G. Wolber, B. Koksch, ACS Chem. Biol. 2014, 9, 613–616.